Summary for iron and oil content Discussion
iron and oil content in zinc phosphate line is discussed as a practical troubleshooting issue rather than a simple lab test. Ashok Surve asks how to find iron and oil content in the acidic degreasing, derusting, and phosphating tanks of a zinc phosphating process. In reply, the answerer suggests the real problem may be poor acidic degreasing or contamination from an overhead hoist dripping oil and rust into the tanks. He notes that oil in the derusting and zinc phosphate tanks would usually be visible as a surface skim, and says progress will be faster if the actual operating situation is described instead of trying to solve it as an abstract analytical question. The response implies that multiple chemical analysis methods would be needed for the different tanks, each with its own interferences, but does not provide a specific test procedure.
February 23, 2014
Q. Please explain how to find Iron and Oil content in Acidic Degreasing, Derusting and Phosphating Tank of Zinc Phosphating Process.
ASHOK SURVE
– Maharashtra, Mumbai, India
Hi Ashok. May I assume that your acidic degreasing step is not working properly, so you think you may be getting oil into your pickling tank and your phosphating tank? Or is an overhead hoist dripping oil and rust into the tanks? I believe that any oil in the derusting tank and zinc phosphate tank would be readily visible as a skim on the surface of the tank.
I am sure we will make progress much faster if you can explain the situation that is confronting you, rather than struggling to pose it as an abstract question that people have rarely if ever faced or thought about, and that would involve at least 6 different chemical analysis techniques (oil and iron analysis in three different types of tanks, each with their own typical interferences to be worked around).
What is actually going on? Thanks.
Regards,

Ted Mooney, P.E.
Striving to live Aloha
finishing.com – Pine Beach, New Jersey
Need quick confidential answers? $25
Need project assistance? $100/hr.
February 2014