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Gold plating of wave guides
I am working for West Virginia University. We have a microwave cavity that needs to be plated with gold (1-2 um).
Maybe it sounds simple for professionals but not for us. We have tried phosphate gold solution (1.3 g KAu(CN)2, 120 g K2HPO4, 30 g KH2PO4 per/L) and current density 1 mA/cm2. The gold layer looks matte and brownish. Is there any way to get a shiny finish without polishing?
We would be glad if you could help us with advice. Thank you.
Alex K [last name deleted for privacy by Editor]- West Virginia, USA
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First, what type of waveguide/cavity material? I'll assume Copper although Aluminum is also possible as well as ferrous based (you did say you were in an edu). The next issue is that of the matte brown finish. Sounds like you're burning the plate. I suggest a Hull cell analysis. Essentially, you plate up on a brass shim that is placed at an angle to the anode. This allows you to compare varying current density to plated appearance. I am also assuming that you are using an appropriate anode w/ appropriate surface area. A platinum coated anode works best although stainless steel can be used for short periods of time without damaging the bath. The surface area of the anode to cathode should be about 1:1 although 2:1 will be ok. Good luck, Jeff Jeff Albom- El Granada, California |
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I would recommend you look at Plasma Enriched Deposition (aka Sputter coating) your university will have this facility I am sure. The film will have better adhesion, better structure and better uniformity.
Vijay Simha- Bangalore, India
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Hi Alex,
Jeff,
Vijay,
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Readers, learn more on similar issues--
letter 49862 proposes a cleaning sequence for copper wave guides that might be applicable. letters 1799, 39679 and 45737 address electroforming of wave guides. letter 49813 is about a cracking problem in plating of copper electroforms. letter 43876 addresses the general issue of making robust copper electroforms. Patient application of the search engine will uncover other related topics.
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Ted Mooney, P.E. finishing.com Brick, New Jersey |